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Investigation of Subboundaries Evolution in Superplastically Deformed NiAl by Positron Lifetime

Xinghao DU , Jianting GUO , Bide ZHOU , Liangyue XIONG

材料科学技术(英)

In order to study the subboundaries evolution in superplastically deformed NiAl, the positron lifetime change during superplastic deformation process was measured. It is shown that the superplastic deformation of NiAl has not influence on its τ2, the newly recrystallized grain boundaries formed during entire superplastic deformation process belong to the calegory of subboundaries and have not contribution to the superplastic strain.

关键词: NiAl , null , null , null

Positron annihilation behaviors and magnetic properties of single-phase Nd2Fe14B and nanocomposite Nd2Fe14B/alpha-Fe magnets

Dingkang XIONG , Xiaokai SUN , Liangyue XIONG , Wei LIU , Tong ZHAO , Zhidong ZHANG

材料科学技术(英)

Positron annihilation behaviors have been studied in the single phase Nd2Fe14B magnet and the nanocomposite Nd2Fe14B/alpha -Fe magnet, prepared by melt spinning. The results showed that the number of vacancy-cluster at grain boundaries increases with increasing annealing temperature for the both types of magnets. The increase of this kind of defect can improve the coercivity of the single-phase magnet. Conversely, the increase of vacancy-cluster amount leads to decreasing of the coercivity for the nanocomposite magnet. It implies that the mechanism of dominant magnetic hardening for the two types of magnets is different, and the domain walls pinning mechanism in the single-phase magnet and the reversal magnetization nucleation mechanism in the nanocomposite magnet operate, respectively.

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Positron lifetime study of the single-phase B2Ni(100-x)Al(x) and Ni50-xCOxAl50 intermetallics

Rongshi CHEN , Jianting GUO , Wenlong ZHOU , Liangyue XIONG

材料科学技术(英)

In order to understand the point defect structure in NiAl Intermetallic compound, the positron lifetime in binary Ni100-xAlx (53 greater than or equal to x greater than or equal to 45) and ternary B2 Ni50-xCoxAl50 (x=0, 5, 10, 15) intermetallic compounds as a function of composition were measured. It is shown that the positron lifetime spectra of these compounds can be consistently expressed by single-component lifetimes. The positron lifetime value in ternary Ni50-xCoxAl50 alloy is independent of Co content and equal to that detected in both stoichiometric and Al-rich NiAl. From an analysis of the present results, it is suggested that the constant lifetime of tau approximate to 180 ps should be ascribed to saturation trapping and annihilation of positron exclusively at Ni vacancy, no evidence for the presence of Al vacancy is available.

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